Synthesis by prato reaction and in situ ultraviolet characterization of several fulleropyrrolidine derivatives

M. A. Jiménez Gómez, M. Garza Castañón, O. V. Kharissova, B. I. Kharisov, U. Ortiz Méndez

Research output: Contribution to journalArticle

1 Citation (Scopus)

Abstract

1-Methyl-2-phenylfulleropyrrolidine (1), 1-methyl-2-(4-(1-piperidyl)-phenyl)- fulleropyrrolidine (2), 1-methyl-2-(4-fluorophenyl)-fulleropyrrolidine (3), and 1-methyl-2-(3-hydroxy- 2-naphtyl)-3,4-fulleropyrrolidine (4) were synthesized by Prato reaction and characterized in situ in the reactionmixture by ultraviolet-visible (UV-vis) spectroscopy, high-performance liquid chromatography (HPLC), and matrix-assisted laser desorption ionization (MALDI). A comparison of theoretical and experimental UV spectra was carried out. Copyright © Taylor & Francis Group, LLC.
Original languageEnglish
JournalInternational Journal of Green Nanotechnology: Materials Science and Engineering
DOIs
Publication statusPublished - 1 Dec 2009
Externally publishedYes

Fingerprint

Ultraviolet visible spectroscopy
High performance liquid chromatography
Ionization
Desorption
Derivatives
Lasers

All Science Journal Classification (ASJC) codes

  • Biomaterials
  • Chemistry(all)
  • Mechanics of Materials

Cite this

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title = "Synthesis by prato reaction and in situ ultraviolet characterization of several fulleropyrrolidine derivatives",
abstract = "1-Methyl-2-phenylfulleropyrrolidine (1), 1-methyl-2-(4-(1-piperidyl)-phenyl)- fulleropyrrolidine (2), 1-methyl-2-(4-fluorophenyl)-fulleropyrrolidine (3), and 1-methyl-2-(3-hydroxy- 2-naphtyl)-3,4-fulleropyrrolidine (4) were synthesized by Prato reaction and characterized in situ in the reactionmixture by ultraviolet-visible (UV-vis) spectroscopy, high-performance liquid chromatography (HPLC), and matrix-assisted laser desorption ionization (MALDI). A comparison of theoretical and experimental UV spectra was carried out. Copyright {\circledC} Taylor & Francis Group, LLC.",
author = "{Jim{\'e}nez G{\'o}mez}, {M. A.} and {Garza Casta{\~n}{\'o}n}, M. and Kharissova, {O. V.} and Kharisov, {B. I.} and {Ortiz M{\'e}ndez}, U.",
year = "2009",
month = "12",
day = "1",
doi = "10.1080/19430840903120094",
language = "English",
journal = "International Journal of Green Nanotechnology: Materials Science and Engineering",
issn = "1943-0841",
publisher = "Taylor and Francis Ltd.",

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Synthesis by prato reaction and in situ ultraviolet characterization of several fulleropyrrolidine derivatives. / Jiménez Gómez, M. A.; Garza Castañón, M.; Kharissova, O. V.; Kharisov, B. I.; Ortiz Méndez, U.

In: International Journal of Green Nanotechnology: Materials Science and Engineering, 01.12.2009.

Research output: Contribution to journalArticle

TY - JOUR

T1 - Synthesis by prato reaction and in situ ultraviolet characterization of several fulleropyrrolidine derivatives

AU - Jiménez Gómez, M. A.

AU - Garza Castañón, M.

AU - Kharissova, O. V.

AU - Kharisov, B. I.

AU - Ortiz Méndez, U.

PY - 2009/12/1

Y1 - 2009/12/1

N2 - 1-Methyl-2-phenylfulleropyrrolidine (1), 1-methyl-2-(4-(1-piperidyl)-phenyl)- fulleropyrrolidine (2), 1-methyl-2-(4-fluorophenyl)-fulleropyrrolidine (3), and 1-methyl-2-(3-hydroxy- 2-naphtyl)-3,4-fulleropyrrolidine (4) were synthesized by Prato reaction and characterized in situ in the reactionmixture by ultraviolet-visible (UV-vis) spectroscopy, high-performance liquid chromatography (HPLC), and matrix-assisted laser desorption ionization (MALDI). A comparison of theoretical and experimental UV spectra was carried out. Copyright © Taylor & Francis Group, LLC.

AB - 1-Methyl-2-phenylfulleropyrrolidine (1), 1-methyl-2-(4-(1-piperidyl)-phenyl)- fulleropyrrolidine (2), 1-methyl-2-(4-fluorophenyl)-fulleropyrrolidine (3), and 1-methyl-2-(3-hydroxy- 2-naphtyl)-3,4-fulleropyrrolidine (4) were synthesized by Prato reaction and characterized in situ in the reactionmixture by ultraviolet-visible (UV-vis) spectroscopy, high-performance liquid chromatography (HPLC), and matrix-assisted laser desorption ionization (MALDI). A comparison of theoretical and experimental UV spectra was carried out. Copyright © Taylor & Francis Group, LLC.

U2 - 10.1080/19430840903120094

DO - 10.1080/19430840903120094

M3 - Article

JO - International Journal of Green Nanotechnology: Materials Science and Engineering

JF - International Journal of Green Nanotechnology: Materials Science and Engineering

SN - 1943-0841

ER -